Operating Instructions Thermo Scientific Barnstead Genpure Water Purification System

Transcript

Operating Instructions Thermo Scientific Barnstead GenPure Water Purification System   Art. No.: 50131211 (Standard)   Art. No.: 50131235 (UF)   Art. No.: 50131217 (UV/UF)   Art. No.: 50131243 (UV)   Art. No.: 50131229 (UV-TOC)   Art. No.: 50131256 (UV-TOC/UF) Serial number: Read these operating instructions carefully before installing and starting the system! 50131265 State: 11.12 Information given is not binding. Rights reserved for technical changes. Thermo Scientific Barnstead GenPure Ultrapure water system EC-Declaration of Conformity in accordance with the EEC machine directive 2006/42/EC, appendix II A We hereby certify that the following described machine in its conception and form put by us into circulation is in accordance with all the relevant essential health and safety requirements of the EC machinery directive 2006/42/EC as amended and the national laws and regulations adopting this directive. This declaration is no longer valid if the machine is modified without our consent. Manufacturer: Thermo Electron LED GmbH Stockland 3 D-56412 Niederelbert Description of the machine: function: Ultrapure water system type: GenPure, GenPure UV, GenPure UV/UF, GenPure UF, GenPure UV-TOC, GenPure UV-TOC/UF article number: 50131211, 50131217, 50131229, 50131235, 50131243, 50131256 The agreement with further valid guidelines/regulations following for the product is explained: EMC Directive (2004/108/EC) Reference to the harmonised standards: DIN EN ISO 12100-1 Safety of machinery, Part 1: Basic terminology DIN EN ISO 12100-2 Safety of machinery, Part 2: Technical principles DIN EN ISO 14121-1 Safety of machinery, Part 1: Risk assessment DIN EN 61326-1 Authorized person for the technical documentation: Detlef Opp Stockland3 D-56412 Niederelbert Niederelbert, 1. April 2010 Detlef Opp, Head of Technical documentation Signature 2 Thermo Scientific Barnstead GenPure Ultrapure water system Preface Dear Sir or Madam Thank you for the confidence you have placed in us by deciding to purchase a GenPure ultrapure water system. You have selected a high quality product designed to give long and reliable service. Before you start to install and commission your GenPure system, please carefully read through the information given in this operating instructions manual on installation and operation. This is important as we, the manufacturer of the system, cannot be held liable for any damage occurring as a result of incorrect operation of it, or use of it for other than the intended purpose. Niederelbert, 1st September 2004 3 Thermo Scientific Barnstead GenPure Ultrapure water system 1. Contents Preface......................................................................................................... 3  1. Contents .................................................................................................. 4  2. Explanatory notes on the operating instructions ..................................... 6  3. Transport and packaging ........................................................................ 7  3.1 Examination on receipt ....................................................................................................... 7  3.2 Complaints ......................................................................................................................... 7  3.3 Packing for return ............................................................................................................... 7 4. Safety precautions .................................................................................. 8  5. Intended purpose .................................................................................. 10  5.1 Application areas .............................................................................................................. 10 6. Parts standardly supplied ...................................................................... 11  7. Technical specifications ........................................................................ 14  8. Description of how the systems function ............................................... 16  8.1 8.2 8.3 8.4 8.5 8.6 Flow chart for GenPure Standard ..................................................................................... 17  Flow chart for GenPure UV .............................................................................................. 18  Flow chart for GenPure UF .............................................................................................. 19  Flow chart for GenPure UV/UF ........................................................................................ 20  Flow chart for GenPure UV-TOC ..................................................................................... 21  Flow chart for GenPure UV-TOC/UF ................................................................................ 22 9. Installation ............................................................................................. 23  9.1 9.2 9.3 9.4 9.5 9.6 The installation area ......................................................................................................... 23  Installing the system ......................................................................................................... 24  Mounting the power pack (voltage supply) ....................................................................... 25  Installation examples ........................................................................................................ 26  Mounting examble GenPure with Ion exchanger DI 1500 (option) ................................... 28  Wall mounting................................................................................................................... 29 10. Putting the system into operation ........................................................ 30  11. The control panel ................................................................................ 31  12. The system control .............................................................................. 32  12.1 The User-menu .............................................................................................................. 33  12.1.1 Feedwater conductivity: ........................................................................................... 33  12.1.2. Ultrapure water limiting value: ................................................................................ 33  12.1.3. UV-Lamp operating time and intensity: ................................................................... 34  12.1.4. Filter cartridge operating hours counter: ................................................................. 34  12.1.5. Rinsing procedure................................................................................................... 34  12.1.6. Disinfection procedure ............................................................................................ 35 4 Thermo Scientific Barnstead GenPure Ultrapure water system   12.1.7 Fault storage display: .............................................................................................. 36  12.1.8 Print-out................................................................................................................... 37  12.1.9 Unlocking the system .............................................................................................. 37 12.2 The OEM-Menu: ............................................................................................................ 39  12.2.1 Set the limiting value for temperature: .................................................................... 39  12.2.2 Set the rinsing time: ................................................................................................ 40  12.2.3 Change the disinfection time: .................................................................................. 40  12.2.4 Set the pump interval time: ..................................................................................... 40  12.2.5 Set the rinse interval time:....................................................................................... 41  12.2.6 Adjust the real time clock: ....................................................................................... 41  12.2.6 Set the sending interval:.......................................................................................... 41  12.2.7 Select the language: ............................................................................................... 42  12.2.8 Switch units, conductivity/resistance: ...................................................................... 42  12.2.9 Switch temperature compensation on/off: ............................................................... 42 12.3 Using volume control for water dispensing .................................................................... 43 12.4 Printer output ................................................................................................................. 43  12.4.1 Standard message .................................................................................................. 43  12.4.2 Code message ........................................................................................................ 44  12.4.3 Error message......................................................................................................... 44 13. Maintenance ....................................................................................... 45  13.1 Maintenance intervals .................................................................................................... 46  13.2 Change the Filter cartridge ............................................................................................ 47  13.3 Disinfection procedure ................................................................................................... 48 14. Waste disposal ................................................................................... 50  15. Trouble shouting................................................................................. 51  16. Replacement parts and consumables ................................................ 54  17. Accessories ........................................................................................ 55  18. Terminal assignment .......................................................................... 57  19. Maintenance record............................................................................ 59  5 Thermo Scientific Barnstead GenPure Ultrapure water system 2. Explanatory notes on the operating instructions EU Mark of Conformity CSA - admission Important operating and/or maintenance instructions! Read the operating instructions with due care. Risk of electric shock! Electrical work on the system is only to be carried out by qualified personnel. General information! Particularly important notes are marked with this information sign. Protective conductor connection Connect the power supply to an electrical socket with a protective connection. The information provided in these operating instructions is only valid for the system which has the serial number which is to be entered on the front page. Please enter the serial number* of your GenPure system in the space provided on the front page. * Read the serial number of your ultra pure water system from the type plate. For quick and correct service, please include the following information on all inquiries and replacement parts orders which relate to your system: - The serial number - The article number 6 Thermo Scientific Barnstead GenPure Ultrapure water system 3. Transport and packaging Ultrapure water systems are carefully controlled and packed, but despite this damage could occur during transport. 3.1 Examination on receipt - Check complete delivery by comparing the parts supplied with those listed in the delivery note. Is the packaging visibly damaged? - Inspect the equipment supplied for damage. 3.2 Complaints Should damage have occurred during transport: - Immediately* contact the postal, railway, shipping or air freight agent. - Save the complete packaging (outer carton and packaging materials) for possible inspection or return delivery. 3.3 Packing for return Whenever possible, use the original carton and packaging material. Should these no longer be available, or be unfit for use: - Pack the equipment in suitable sheets or bags in a strong cardboard box so that all parts are protected against shock. * The time limit for claims is 6 days after the date of delivery. All rights to claim for damages cease when this time limit has elapsed. 7 Thermo Scientific Barnstead GenPure Ultrapure water system 4. Safety precautions For your own safety, please observe the above safety precautions! 8  Your GenPure system is an advanced system that has been designed exclusively for the production of ultrapure water from potable water that has been pretreated by reverse osmosis, ion exchange or distillation.  Do not start to install or operate the system until you have heeded the corresponding information contained in these Operating Instructions.  Lifting and carrying the ultra pure water system, e.g. to the installation location, should be carried out by two people. To lift it, each takes hold of it under the base plate at two corners.  Do not make changes to the system. Please note that the manufacturer’s liability does not cover damages resulting from improper operation or from use other than for the intended purpose.  The CE-mark is invalidated when constructional changes are made to the system or foreign products are installed in it.  Protect the system from frost. The temperature at the installation area must not go below +2°C.  Follow all general regulations and requirements that must be observed at the installation location, including the valid accident prevention regulations.  A feedwater pressure of min. 0.1 bar and max. 6 bar is required. Install an additional pressure reducer should the feedwater pressure be higher.  DIN EN 1717 requires that water purification systems be equipped with a safety device that protects the drinking water system from contamination.  A grounded 100-240V, 50/60Hz socket must be available.  A floor drain with at least DN 50 pipe (38.5 mm internal diameter) must be available at the installation area.  When the system is to be wall-mounted, check the statics of the wall for sufficient load-bearing capacity (see Technical Data for the weight of your system). The ultrapure water system only be mounted on a concrete wall or a solid masonry.  Positioning the system so that operation of the power separation unit is not made difficult.  The maximum operating temperature is +40°C. Thermo Scientific Barnstead GenPure Ultrapure water system  When the system will be at a standstill for a longer period (e.g.long holidays), proceed as follows:  Switch the system off.  Close the supply of feedwater to the ultrapure water system. Damage to the pump will occur should the supply of feedwater be turned off with the system still on. The manufacturer does not accept liability should such damage occur.  When planning the installation of the system, ensure that there will be sufficient working room for convenient operation of the system and for maintenance such as changing the Filter cartridge and opening, breaking and checking connections.  The guarantee is valid for a period of 12 months.  Never look directly at a switched-on UV-lamp, because UV light endangers eyesight! Never switch the UV-lamp on when is has been taken out of the metal cylinder! Only authorized personnel are to carry out UV-lamp replacement. 9 Thermo Scientific Barnstead GenPure Ultrapure water system 5. Intended purpose Increasingly sophisticated technologies, continually lower detection limits in laboratory analysis, and the requirement for biologically-pure water in research correspondingly require the water used to be of ever higher quality. The novel GenPure line of water purification systems has been developed to produce such ultrapure water, as well as to fill the needs for user-friendly systems and complete solutions GenPure ultrapure water systems produce salt-free, organically-pure particle-free and sterile filtered ultrapure water. To make full use of the long and economical service life of the high-quality purification media, the feedwater for GenPure systems must be pretreated by an appropriate purification step (reverse osmosis, ion exchange or distillation. 5.1 Application areas - Analytical methods: - HPLC - IC - ICP - AAS - TOC-measurements - DNA research - etc. (High Performance Liquid Chromatography) (Ion Chromatography) (Inductive Coupled Argon Plasma ) (Atomic Absorptions Spectrophotometry) (Total Organic Carbon) - Preparation of reagents and solutions: - Cell culture media - Tissue culture media - Make-up water for reagents for online analyzers - Ultraclean washing and rinsing processes in laboratories 10 Thermo Scientific Barnstead GenPure Ultrapure water system 6. Parts standardly supplied The following GenPure versions are available: GenPure Standard GenPure UF GenPure UV GenPure UV/UF GenPure UV-TOC GenPure UV-TOC/UF (Standard system) (Standard system + Ultrafiltration module) (Standard system + UV-photooxidation) (Standard system + UV-photooxidation + Ultrafiltration module) (Standard system + UV-photooxidation with TOC-measurement) (Standard system + UV-photooxidation with TOC-measurement + Ultrafiltration module) (Please check that the version you have received corresponds to that stated on the delivery note.) Art.-No. 50131211 consists of: GenPure Standard basic unit Material for wall-mounting Connecting hose, 1.5 m, straight/angle Sterile filter capsule, 0.2 µm Filter cartridge for ultrapure water systems PE hose, 8 mm OD, 2 m Operating Instructions manual Connecting cord (rubber connector to nema plug connector) Connecting cord (rubber connector to british ST plug connector) Connecting cord (rubber connector to euro plug connector) Tabletop power pack Universal adapter Universal holder (Article-No. 18.0042) (Article-No. 09.1003) (Article-No. 09.2005) (Article-No. 18.0036) (Article-No.50131265) (Article-No. 50132200) (Article-No. 50132203) (Article-No. 50132215) (Article-No. 50134196) (Article-No. 21.1006) (Article-No. 21.1007) Art.-No. 50131235 consists of: GenPure UF basic unit Material for wall-mounting Connecting hose, 1.5 m, straight/angle Sterile filter capsule, 0.2 µm Filter cartridge for ultrapure water systems PE hose, 8 mm OD, 2 m Operating Instructions manual Connecting cord (rubber connector to nema plug connector) Connecting cord (rubber connector to british ST plug connector) Connecting cord (rubber connector to euro plug connector) Tabletop power pack Universal adapter Universal holder (Article-No. 18.0042) (Article-No. 09.1003) (Article-No. 09.2005) (Article-No. 18.0036) (Article-No. 50131265) (Article-No. 50132200) (Article-No. 50132203) (Article-No. 50132215) (Article-No. 50134196) (Article-No. 21.1006) (Article-No. 21.1007) 11 Thermo Scientific Barnstead GenPure Ultrapure water system Art.-No. 50131243 consists of: GenPure UV basic unit Material for wall-mounting Connecting hose, 1.5 m, straight/angle Sterile filter capsule, 0.2 µm Filter cartridge for ultrapure water systems PE hose, 8 mm OD, 2 m Operating Instructions manual Connecting cord (rubber connector to nema plug connector) Connecting cord (rubber connector to british ST plug connector) Connecting cord (rubber connector to euro plug connector) Tabletop power pack Universal adapter Universal holder (Article-No. 18.0042) (Article-No. 09.1003) (Article-No. 09.2005) (Article-No. 18.0036) (Article-No. 50131265) (Article-No. 50132200) (Article-No. 50132203) (Article-No. 50132215) (Article-No. 50134196) (Article-No. 21.1006) (Article-No. 21.1007) Art.-No. 50131217 consists of: GenPure UV/UF basic unit Material for wall-mounting Connecting hose, 1.5 m, straight/angle Sterile filter capsule, 0.2 µm Filter cartridge for ultrapure water systems PE hose, 8 mm OD, 2 m Operating Instructions manual Connecting cord (rubber connector to nema plug connector) Connecting cord (rubber connector to british ST plug connector) Connecting cord (rubber connector to euro plug connector) Tabletop power pack Universal adapter Universal holder (Article-No. 18.0042) (Article-No. 09.1003) (Article-No. 09.2005) (Article-No. 18.0036) (Article-No. 50131265) (Article-No. 50132200) (Article-No. 50132203) (Article-No. 50132215) (Article-No. 50134196) (Article-No. 21.1006) (Article-No. 21.1007) Art.-No. 50131229 consists of: GenPure UV-TOC basic unit Material for wall-mounting Connecting hose, 1.5 m, straight/angle Sterile filter capsule, 0.2 µm Filter cartridge for ultrapure water systems PE hose, 8 mm OD, 2 m Operating Instructions manual Connecting cord (rubber connector to nema plug connector) Connecting cord (rubber connector to british ST plug connector) Connecting cord (rubber connector to euro plug connector) Tabletop power pack Universal adapter Universal holder 12 (Article-No. 18.0042) (Article-No. 09.1003) (Article-No. 09.2005) (Article-No. 18.0036) (Article-No. 50131265) (Article-No. 50132200) (Article-No. 50132203) (Article-No. 50132215) (Article-No. 50134196) (Article-No. 21.1006) (Article-No. 21.1007) Thermo Scientific Barnstead GenPure Ultrapure water system Art.-No. 50131256 consists of: GenPure UV-TOC/UF basic unit Material for wall-mounting Connecting hose, 1.5 m, straight/angle Sterile filter capsule, 0.2 µm Filter cartridge for ultrapure water systems PE hose, 8 mm OD, 2 m Operating Instructions manual Connecting cord (rubber connector to nema plug connector) Connecting cord (rubber connector to british ST plug connector) Connecting cord (rubber connector to euro plug connector) Tabletop power pack Universal adapter Universal holder (Article-No. 18.0042) (Article-No. 09.1003) (Article-No. 09.2005) (Article-No. 18.0036) (Article-No. 50131265) (Article-No. 50132200) (Article-No. 50132203) (Article-No. 50132215) (Article-No. 50134196) (Article-No. 21.1006) (Article-No. 21.1007) 13 Thermo Scientific Barnstead GenPure Ultrapure water system 7. Technical specifications Source and treatment Colloid index (SDI) Feedwater resistance Free chlorine TOC Bacteria Turbidity Carbon dioxide (CO2) Silicate Particles Temperature Pressure Required quality of the feedwater Potable water that has been pretreated by reverse osmosis, ion exchange or distillation. max. 1 for all versions. Additional upstream 1 µm membrane filtration is recommended for feedwater that has not been pretreated by reverse osmosis. > 0.5 MΩxcm max. 0.05 ppm max. 50 ppb < 100 CFU/ml < 1.0 NTU max. 30 ppm max. 2 ppm Filtration to 0.2 µm is recommended to protect internal media and filters from fine particles. 2 - 35 °C 0.1 - 6 bar Product water quality Resistance (Reference temperature 25°C) TOC Bacteria Bacterial Endotoxines Particles Flow rate Flow rate with volume control Standard UV UF UV/UF UV-TOC UVTOC/UF MΩxcm at 25°C 18.2 18.2 18.2 18.2 18.2 18.2 ppb CFU/ml 5 - 10 <1 1-5 <1 5 - 10 <1 1-5 <1 1-5 <1 1-5 <1 -- -- < 0.001* < 0.001* -- < 0.001* < 1/ml up to 2 < 1/ml up to 2 < 1/ml up to 1.7 < 1/ml up to1.7 < 1/ml up to 2 < 1/ml up to 1.7 1.2 1.2 1.2 1.2 1.2 1.2 EU/ml > 0.2 µm L/min** L/min * Depending on feedwater and appropriate disinfection ** Depending on feedwater pressure Height Width Depth Weight: GenPure Standard GenPure UF GenPure UV GenPure UV/UF GenPure UV-TOC GenPure UV-TOC/UF Dimensions and weight 615 mm 372 mm 330 mm 22 kg 23 kg 24 kg 24 kg 24 kg 25 kg Cell constants of the measuring cells Feedwater conductivity 0.16 cm-1 Conductivity after UV-oxidation 0.01 cm-1 Ultrapure water conductivity 0.01 cm-1 14 Thermo Scientific Barnstead GenPure Ultrapure water system Feedwater Rinse water Ultrapure water Sterile filter outlet Connectors for water R 3/4" 8 mm OD hose R 1/4" 8 - 10 mm OD hose Electrical connections / external switched mode power supply Input voltage AC 100 – 240 V, 50 – 60 Hz, 5 – 3.8 A Output voltage DC 24 V, 3.8 A System connection DC 24 V, 80 W Serial interface RS 232 Protection Class Class II (external SMPS certified as Class I) Airborne sound emission Sound-pressure level 49 db(A) Ambient conditions (DIN EN 61010-1 (VDE 0411-1):2011-02) Usage Indoor rooms Height Up to 2000 m Temperature range From 5° C to 40° C Relative humidity Maximum relative humidity 80 % at temperatures of up to 31° C, linearly decreasing to 50 % relative humidity at 40° C Line-voltage variation Not more than ± 10 % of the line voltage Transient overvoltages As usually occur in the supply network (overvoltage category II acc. to IEC 60364-4-443). Note: The rated level of transient overvoltage is the withstand impulse voltage acc. to overvoltage category II of IEC 60364-4-443 Ventilation requirements There are no special requirements with regard to ventilation. Degree of pollution 2 Materials of parts that contact water Pressure reducer NBR Pump head Nylon with glass fibre UV-Lamp Ultrapure quartz UV-Housing Stainless steel Ion exchanger PP UF-Housing Polycarbonate Rinsing solenoid valve PA Dispensing valve PVDF Conductivity measuring cell POM, stainless steel Distributor block POM Connectors POM Hoses PE Gaskets EPDM 15 Thermo Scientific Barnstead GenPure Ultrapure water system 8. Description of how the systems function GenPure Standard, UV, UF and UV/UF versions Potable water is pretreated by a downstream reverse osmosis, ion exchange system or distillation, then fed through a pressure reducer into the GenPure ultrapure water system, where the conductivity of it is measured. A pump forces this feedwater through a UV-photooxidation (only with GenPure UV and GenPure UV/UF) and a Filter cartridge, then through an ultrafiltration module. (only with GenPure UF and GenPure UV/UF), following which the conductivity is permanently measured by a special measuring cell (with temperature compensation). When the dispensing valve is opened, the ultrapure water is subjected to filtration by a sterile filter immediately prior to flowing out of the ultrapure water outlet. When the system is in stand-by mode (the Interval operating state), the water in the system is recirculated through the internal circuit at regular intervals. GenPure UV-TOC and UV-TOC/UF versions Potable water is pretreated by a downstream reverse osmosis, ion exchange system or distillation, then fed through a pressure reducer into the GenPure ultrapure water system, where the conductivity of it is measured. A pump forces this feedwater through a UV-photooxidation, following which the conductivity of the water is measured for the TOC determination, and on through a Filter cartidge and an ultrafiltration module (only with GenPure UV-TOC/UF), and the conductivity is then permanently measured by a special measuring cell (with temperature compensation). The TOC value is calculated by taking the difference between the values measured by the measuring cells QIA300 and QI302. The measurement range is 0 - 30 ppb. When this measurement range is exceeded, the number 99 is shown in the display instead of the measured value. In Stand-by operation, "___" is shown instead of the measured value. When the dispensing valve is opened, the ultrapure water is subjected to filtration by a sterile filter immediately prior to flowing out of the ultrapure water outlet. When the system is in standby mode (the Interval operating state), the water in the system is recirculated through the internal circuit at regular intervals. 16 Thermo Scientific Barnstead GenPure Ultrapure water system 8.1 Flow chart for GenPure Standard A-F1 A-F2 A-P1 QIA 300 QIA 303 TIA 500 V1 V2 V3 V4 Filter cartridge Sterile filter Circulation pump Feedwater conductivity measuring cell Ultrapure water conductivity measuring cell Temperature sensor Pressure reducer Check valve Dispensing valve Rinsing solenoid valve 17 Thermo Scientific Barnstead GenPure Ultrapure water system 8.2 Flow chart for GenPure UV A-F1 A-F2 A-P1 A-UV1 QIA 300 QIA 303 TIA 500 V1 V2 V3 V4 18 Filter cartridge Sterile filter Circulation pump UV-photooxidation Feedwater conductivity measuring cell Ultrapure water conductivity measuring cell Temperature sensor Pressure reducer Check valve Dispensing valve Rinsing solenoid valve Thermo Scientific Barnstead GenPure Ultrapure water system 8.3 Flow chart for GenPure UF A-F1 A-F2 A-F3 A-P1 QIA 300 QIA 303 TIA 500 V1 V2 V3 V4 Filter cartridge Sterile filter Ultrafiltration module Circulation pump Feedwater conductivity measuring cell Ultrapure water conductivity measuring cell Temperature sensor Pressure reducer Check valve Dispensing valve Rinsing solenoid valve 19 Thermo Scientific Barnstead GenPure Ultrapure water system 8.4 Flow chart for GenPure UV/UF A-F1 A-F2 A-F3 A-P1 A-UV1 QIA 300 QIA 303 TIA 500 V1 V2 V3 V4 20 Filter cartridge Sterile filter Ultrafiltration module Circulation pump UV-photooxidation Feedwater conductivity measuring cell Ultrapure water conductivity measuring cell Temperature sensor Pressure reducer Check valve Dispensing valve Rinsing solenoid valve Thermo Scientific Barnstead GenPure Ultrapure water system 8.5 Flow chart for GenPure UV-TOC A-F1 A-F2 A-P1 A-UV1 QIA 300 QIA 301 QI 302 QIA 303 TIA 500 V1 V2 V3 V4 Filter cartridge Sterile filter Circulation pump UV-photooxidation Feedwater conductivity measuring cell UV-Intensity Conductivity for TOC-measurement Ultrapure water conductivity measuring cell Temperature sensor Pressure reducer Check valve Dispensing valve Rinsing solenoid valve 21 Thermo Scientific Barnstead GenPure Ultrapure water system 8.6 Flow chart for GenPure UV-TOC/UF A-F1 A-F2 A-F3 A-P1 A-UV1 QIA 300 QIA 301 QI 302 QIA 303 TIA 500 V1 V2 V3 V4 22 Filter cartridge Sterile filter Ultrafiltration module Circulation pump UV-photooxidation Feedwater conductivity measuring cell UV-Intensity Conductivity for TOC measurement Ultrapure water conductivity measuring cell Temperature sensor Pressure reducer Check valve Dispensing valve Rinsing solenoid valve Thermo Scientific Barnstead GenPure Ultrapure water system 9. Installation 9.1 The installation area The following criteria must be considered when the installation area is selected:  Feedwater pressure at least 0.1 bar, at most 6 bar. The feedwater pressure must not exceed 6 bar. With higher pressures, a pressure reducer must be installed.  Minimum temperature +2°C  Level standing surface   The standing surface or the wall where the system is to be stood or mounted must have sufficient weight-bearing capacity (see Technical specifications for weight). The ultrapure water system only be mounted on a concrete wall or a solid masonry.  DN 50 floor drain  Unrestricted gravity fall to the floor drain. Should a floor drain not be available, install a Water Watcher (Article No.: 16.0129) to protect against water damage! A free flow-off must be ensured!  Grounded 100-240 V, 50/60 Hz socket  Positioning the system so that operation of the power separation unit is not made difficult.  Sufficient working room around the GenPure system (for Filter cartridge change, etc.)  The system must be positioned for easy operation and control  R 3/4" potable water tap connection 23 Thermo Scientific Barnstead GenPure Ultrapure water system 9.2 Installing the system 1) Feedwater inlet connector, R 3/4" male thread 2) Rinsing water outlet connector, 8 mm OD 3) Connector for an optional printer (Article No.: 16.0330) Proceed as follows to prepare your GenPure ultrapure water system for operation: 24  Stand the GenPure system on the selected surface or hang it on the wall using the hooks supplied.  Remove the cartridge cover from the GenPure system (push-button on the top).  Remove the closing caps from the Filter cartridge and save them for later use.  Push the Filter cartridge in (guide in the recess), fit the quick-connect couplings on and put the cover back on.  Fit the connecting hose to the GenPure system (connector 1) and to the feedwater connector (see the following Installation examples)  Use the 8 mm OD hose to connect the GenPure system (connector 2) to the floor drain, ensuring free gravity fall to drain. The drain to the sewer must be max. Are 1m above the rinsing water connector of the Unit.  If not already fitted, screw the sterile filter provided into the R 1/4" female thread of the dispensing valve outlet.  Plug the line cord into an earthed 100-240, 50/60 Hz socket.  Open the feedwater tap. Thermo Scientific Barnstead GenPure Ultrapure water system 9.3 Mounting the power pack (voltage supply)  Whenever possible, mount the power pack on the wall to the left or right of the ultra pure water system where it is freely accessible.  Stick the universal holder which is supplied in the assembly kit to the back of the power pack as shown in the above Figure.  Stick the universal adapter to a smooth wall surface or screw it to the wall using the dowels and screws supplied in the assembly kit.  When the universal holder and universal adapter have been fitted, hang the power pack in.  Plug the connecting cable (appliance cable) in the power pack socket.  Connect the power pack to the ultra pure water system (4-pin power supply connector,).  The system is now ready for use. 25 Thermo Scientific Barnstead GenPure Ultrapure water system 9.4 Installation examples Connection to a pretreatment unit: Connection to a Pacific TII/TII UV system with a storage tank: 26 Thermo Scientific Barnstead GenPure Ultrapure water system Connection to a storage tank: Caution: When connected to a storage tank, the GenPure system must be switched to "Nonstop" operation when ultrapure water is to be dispensed. 27 Thermo Scientific Barnstead GenPure Ultrapure water system 9.5 Mounting examble GenPure with Ion exchanger DI 1500 (option) Proceed as follows to connect an ion exchanger to the upstream side of the GenPure system: 28 1) Connect the hose wich has a R3/4 union nut (1) from the raw water tap to the R3/4” input of the ion exchanger. 2) Make connection from the R3/4 output of the ion exchanger to the feedwater Connector of the GenPure system by using the feedwater connector kit (2) that is contained in the assembly kit (article no. 50136423) Thermo Scientific Barnstead GenPure Ultrapure water system 9.6 Wall mounting Proceed as follows to mount your GenPure system to a wall:  Use a twist drill (8 mm diameter or 5/16 inch) to make the two holes in the wall that are required as shown in the diagram above.  Plug the nylon S8 dowel that are supplied in the assembly kit in the holes. Screw the 5.2 x 50 mm screw hooks that are also supplied in the assembly kit in the dowels.  Lift the GenPure system (2 people are required for this) and hang the back side of it on the screw hooks. 29 Thermo Scientific Barnstead GenPure Ultrapure water system 10. Putting the system into operation Allow the system to warm up to, or to cool down to, room temperature before starting it up for the first time. Check that all hose connections have been made as specified in the "Setting up the system" section. Switch the system on by pressing this button. After a compulsory rinse the system switches to the last operating mode. To vent air from the system, switch the system 3 times successively to "Rinsing" in the menu and collect and discard approx. 5 litres of water each time. The ultra pure water limiting value can be gone below during this procedure. Use this “NONSTOP“-key to switch the system to the “Nonstop“ operating mode. You can set the system back to “Interval“ operation when the system has brought the ultra pure water to the quality you require. 30 Thermo Scientific Barnstead GenPure Ultrapure water system 11. The control panel Intervall – ppb 18,2 MΩxcm 18,5°C UV/TC 31 Thermo Scientific Barnstead GenPure Ultrapure water system 12. The system control General information A single press on the ON/OFF-key brings the system to the Interval operating state (see Interval operation). In this stand-by mode, recirculation within the system is automatically started every half hour, and lasts for the time set. This measure assures maintenance of the ultrapure water quality. The text message "UV" indicates that the UV-lamp is switched on. The text message "TC" indicates that temperature compensation is switched on. In addition, the measured value of the ultrapure water and the temperature are displayed. Should a fault occur, the corresponding fault message is transmitted via the potential-free output and is shown in clear text in the 4th line of the display. In the case of several faults occurring at one time, they are alternately shown in the display. A press on the NONSTOP-key switches the system to Nonstop operation. The pump runs and the rinsing solenoid valve opens for the duration of the Rinse interval that has been set. A press on the INTERVAL-key stops Nonstop operation and switches the system to Interval operation. After 2 hours, the system switches itself automatically to Interval operation When the UV-key is pressed, "UV" is shown in the display, but the UV-lamp is only actuated when the system is in the Nonstop operation state. It is automatically switched off when Nonstop operation is stopped after 2 h. When Nonstop operation is manually stopped by pressing the INTERVAL-key, the UV-lamp is not switched off until it has been burning for a minimum of 0.5 hours. The intensity of the UV-light is monitored when the UV-lamp is actuated, and the measured value is shown in the display. The TOC-value is additionally shown. The User-menu All measured values, operating times and limiting values that are relevant for the user can be set and read here. A press on the menu-key brings you into this menu. Each further press on the menu-key moves you from one menu point to the next. Settings can be changed by pressing on the arrow-keys and be confirmed by pressing the enter-key, which also takes you to the next menu point. Settings can only be changed when the system control has been previously unlocked (see 12.1.8). To simplify changing a value, a press on the UV-key allows you to select the position in a number which you wish to change, and then use the arrow keys to replace the digit there by any digit from 0 - 9. Minimum and maximum measured values have been entered as limiting values in the fixed programme for each of the conductivity and temperature measuring cells. Should these measured values be gone below or exceeded, it can be assumed that a break in a cable has occurred. The fault message "Meas.cell LF1", "Meas. cell LF2", "Meas. cell LF3" or "Temp. Meas. cell" is shown in the 4th line of the display. 32 Thermo Scientific Barnstead GenPure Ultrapure water system 12.1 The User-menu 12.1.1 Feedwater conductivity: A single press on the menu-key allows the feedwater conductivity to be read or the limiting value of it to be changed. The fault message „Limit value feed“ flashes in the 4th line of the display when the limiting conductivity value is exceeded. Feedwater measuring range: 10 – 0.01 MΩxcm Limiting value setting range: 0.1- 50.0 µS/cm Basic setting: 0.5 MΩxcm When a setting above 50 µS/cm/ 0.02 MΩxcm is entered for the limiting value, the limiting value is switched off and the word „Off“ appears in the display. The display shows: Feedwater 1.25 MΩxcm Limit value feed 2.0 µS/cm 12.1.2. Ultrapure water limiting value: Two presses on the menu-key in this menu allow the fault display for the pure water limiting value and the pure water limiting value to be set. As soon as the fault display is switched on, the fault will be displayed both in Stand-by mode and in Production mode. When the fault display is switched off, the fault is only displayed in Production mode. The “Lim. val.pure w.” message is displayed when the limiting value is exceeded. Ultrapure water measuring range: 0.1 MΩxcm Limiting value setting range: 0.055- 5.000 µS/cm Basic setting: 10 MΩxcm Basic setting, fault suppression: On When a setting above 5.0 µS/cm is entered for the limiting value, the limiting value is switched off and the word „Off“ appears in the display. The display shows: Fault message Stand- by On Lim. val. pure w. 0.100 µS/cm 33 Thermo Scientific Barnstead GenPure Ultrapure water system 12.1.3. UV-Lamp operating time and intensity: In this menu the operation hours of the UV-lamp are indicated and the evaluation of UVsensor input into the display under “UV time”. The fault message "UV duration" is displayed when the maximum operating time has been reached. The UV-sensor measures the intensity of the UV-light, and this is displayed as a percentage value of the maximum value. The display shows: UV time 0000 h UV intensity 90% 12.1.4. Filter cartridge operating hours counter: After fourth press on the menu-key the operating hours counter for the filter cartridge is set by input of a valid serial number. The display shows: Ser. no.: cartridge Press enter -----/-12.1.5. Rinsing procedure A fifth press on the menu-key calls the question asking if rinsing is to be carried out. A press on the enter-key confirms this and triggers the rinsing procedure. The pump starts and the rinsing solenoid valve opens for the rinsing time set in the OEM-menu. The remaining rinsing time is shown in the display during rinsing Neither fault messages nor measured values are displayed during rinsing. When the rinsing procedure is finished, the system returns to the last operating state (Interval or Nonstop). The display shows: Rinse ? Press enter 34 Thermo Scientific Barnstead GenPure Ultrapure water system The display during rinsing: Rinse 30 sec. 12.1.6. Disinfection procedure A sixth press on the menu-key calls the question asking if a disinfection is to be carried out. A press on the enter-key confirms this, following which the demand “Disinfection cartridge must be fitted” is shown. When this has been fitted, a confirming press on the enter-key triggers the disinfection procedure. The pump starts for the full time set in the OEM-menu and, when the half of this time has elapsed, the rinsing solenoid valve opens and stays open until the disinfection procedure has finished. The demand "New Filterset must be fitted" is then displayed. When this has fitted, confirmation with the enter-key causes the system to return to the last operating state. During disinfection the remaining disinfection time is shown in the display. The display shows: Disinfection Press enter The display after confirmation with the enter-key: Disinfection cartridge Press enter ! The display during the disinfection procedure: Disinfection 25 min. 35 Thermo Scientific Barnstead GenPure Ultrapure water system The display when disinfection has been completed: New filterset Press enter 12.1.7 Fault storage display: A seventh press on the menu-key calls the fault storage, and the contents of this can be examined by pressing the Enter-key. Up to two faults are shown in the display, each with the date and time at which they occurred. Pressing the appropriate arrow key allows any fault messages before or after those shown to be called. A press on the menu-key or on the Enter-key returns the system to the last operating state. The display shows: Error history Press enter The fault storage display: 14.03.04 14.30 Limit value feed 14.03.04 15.30 Lim. value pure w. 36 Thermo Scientific Barnstead GenPure Ultrapure water system 12.1.8 Print-out A eight press on the menu-key bring you to a menu in which you can hand-request a printout. The display shows: Print out? Press enter 0000 12.1.9 Unlocking the system A nine press on the menu-key calls the menu „Code". To prevent unauthorized access to the settings, changes to settings can only be made when a correct code number from the following Table is entered and confirmed with Enter. The unlocking is then active for a 5 minute period. Each access via the code is printed out by the printer (RS 232) complete with date, time and shortened code number. ("Code 150" = Code 0001, "Code 250" = Code 0002 etc.) The display shows: Code Press enter 0000 You can assign the permissible code numbers listed in the Table on the following page to appropriate members of the staff etc. When names have been entered, tear the page out and file it where it is safe from unauthorized viewing. 37 Thermo Scientific Barnstead GenPure Ultrapure water system Table for assigning permissible code numbers for unlocking the system Code-No. 150 250 350 450 550 650 750 850 950 38 printed out 0001 0002 0003 0004 0005 0006 0007 0008 0009 Person Thermo Scientific Barnstead GenPure Ultrapure water system 12.2 The OEM-Menu: Basic settings and limiting values can be changed in this menu. To make such changes in the OEM-menu, the system must first be unlocked (see 12.1.7). Calling the OEM-menu: Simultaneous presses on the INTERVAL-key and the NONSTOP-key call the OEM-menu. The display shows "OEM-Menu Press enter!“. On confirming this by pressing the enterkey, the first menu point is called to be worked on. To simplify making changes, a press on the UV-key allows the position that is to be changed in a number to be selected, so that the arrow keys can be used to replace it with any digit from 0 – 9. A press on the menu-key takes you to the next menu point. The display shows: OEM-Menu Press enter 12.2.1 Set the limiting value for temperature: The maximum operating temperature limit for the system iss et here. Should this temperature be exceeded, the fault message „Max. temperature" is triggered. This is shown in the 4th line of the display. Basic setting: Setting range: 50 °C 1 - 50 °C The display shows: OEM-Menu Max. temp. 35 °C 39 Thermo Scientific Barnstead GenPure Ultrapure water system 12.2.2 Set the rinsing time: Basic setting: Setting range: 30 sec. 10 - 60 sec. The display shows: OEM-Menu Rinse time 30 sec. 12.2.3 Change the disinfection time: Basic setting: Setting range: 30 min. 15 - 90 min. The display shows: OEM-Menu Disinfect. time 30 min. 12.2.4 Set the pump interval time: Basic setting: Setting range: 5 min. 1 - 30 min. The display shows: OEM-Menu Pump interval 5 min. 40 Thermo Scientific Barnstead GenPure Ultrapure water system 12.2.5 Set the rinse interval time: Basic setting: Setting range: 0.5 sec. 0.1 - 2 sec. The display shows: OEM-Menu Rinse interval 0.5 sec. 12.2.6 Adjust the real time clock: Basic setting: Setting range: The actual date Month 1 - 12, Day 1 - 31, Hour 0 - 24, Minutes 0 - 60. The display shows: OEM-Menu Day 30 Month 12 Year 2003 Hour 12 min. 30 12.2.6 Set the sending interval: The sending interval at which measured values and fault messages are transmitted via the RS 232 interface can be set here. Basic setting: Setting range: 1 hour 0.5 - 12 hours The display shows: OEM-Menu Send interval 1h 41 Thermo Scientific Barnstead GenPure Ultrapure water system 12.2.7 Select the language: Basic setting: Setting range: German German, English, French The display shows: OEM-Menu Language English 12.2.8 Switch units, conductivity/resistance: Basic setting: Setting range: Resistance MΩxcm Resistance MΩxcm, specific electrical resistance MΩ cm The display shows: OEM-Menu µS/cm / MΩxcm MΩxcm 12.2.9 Switch temperature compensation on/off: Basic setting: Setting range: On On, Off The display shows: OEM-Menu Temp. comp. On 42 Thermo Scientific Barnstead GenPure Ultrapure water system 12.3 Using volume control for water dispensing GenPure systems that are equipped with the option of volume control allow volumecontrolled dispensing to be carried out. As soon as the Nonstop operating mode is selected, the number of litres that were last required appears as set value in line 2 of the display. Press once on the Enter-key if you wish to use the arrow keys to change this set value within the permissible range of 0.01 to 60 litres. You can use the UV-key to position the cursor at the position where you want to change the number. Press twice on the Enter-key if you wish to have the displayed water volume dispensed. During dispensing, the number shows the actual volume dispensed. Dispensing is stopped as soon as the set value has been reached. Dispensing can be stopped at any time by a further press on the Enter-key. To carry out manual dispensing of volumes smaller than the set value, first press the Enter-key twice, then press it once again when the required volume has been dispensed. The Display shows: Non-Stop 5 ppb 18.2 MΩxcm 1,00L 21,3°C UV/TC 12.4 Printer output By means of the printer different parameters are documented. It is differentiated between three messages. - Standard message - Code message - Error message 12.4.1 Standard message Here in dependence of the transmit interval of all measured values are printed out. Within the NONSTOP-operation a complete data record is printed out. 43 Thermo Scientific Barnstead GenPure Ultrapure water system Printout: e. g.: 27.02.07 15:15 GenPure Standard S.No. 3988/07 Interv. TC on UV off LF1= 18.2 MΩxcm LF2= 10.0 MΩxcm LF3= 0.000 MΩxcm Temp.= 16.8 °C TOC= 0 ppb UV Intens.= 0% Standard protocol contains all measured values. With devices without TOC measurement and UV-intensity are spent the measured values with 0! 12.4.2 Code message If a code number is entered into the system control and confirmed with the enter key, then the code input is printed out immediately. Code identification (see „tables of classification for authority codes for unlocking the system“). Printout: e. g.: 27.02.07 15:17 GenPure Standard S.No. 3988/07 Code 0002 12.4.3 Error message If an error message in the display, e.g. the high-purity water limit value is indicated, the error message is printed out after the transmit interval. Printout: e. g.: 44 27.02.07 17:09 GenPure Standard S.No. 3988/07 Reinst.grenzwert Thermo Scientific Barnstead GenPure Ultrapure water system 13. Maintenance Regular maintenance maintains the value of your system. We recommend that you close a service contract with representative authorized to service your area. You then have the certainty that your system is kept at a high level of operational safety and reliability. NOTE! To ensure your system will work reliably for a long time, it must be controlled, maintained and cared for at regular intervals in accordance with the information given in these operating instructions! These operating instructions must therefore be kept readily available to operating and maintenance staff at all times, and the staff must carefully follow them! Any maintenance work that is necessary during the period of the guarantee is only to be carried out by a customer service company expressly authorized to do this. It is the duty of the operating staff to carry out the weekly controlling of the system. During the period agreed upon for the guarantee, maintenance is to be carried out weekly according to the maintenance record provided in this operating instruction manual. IMPORTANT! Ion exchangers should be replaced when the ultrapure water limiting value is exceeded. Longer usage can be result in bacterial growth on the resin. Sanitization of the system by the performance of rinsing and disinfection is carried out for reasons of hygiene and has no effect on the technical condition of the system. The system need only be rinsed and disinfected when algae or slime is determined in it, otherwise at least once per year. Prior to carrying out control or maintenance work on electrical equipment, the mains power supply must be switched off and protected against being unwantedly switched on again. Such work is only to be performed by assigned skilled technicians. 45 Thermo Scientific Barnstead GenPure Ultrapure water system 13.1 Maintenance intervals Consumable materials are to be replaced at the intervals given in the following Table or when there is a drop in performance: Material Filter cartridge Sterilefiltercapsule Ultrafiltration membrane Flow chart no. Article no. Interval* F1 F2 F3 09.2005 09.1003 50133980 12 Months 12 Months 24 Months *Please keep in mind that the life of your consumables is directly dependent on the quality of the feed water and the amount of water used daily. The interval is contingent on the feedwater quality so that a shorter one may be necessary. 46 Thermo Scientific Barnstead GenPure Ultrapure water system 13.2 Change the Filter cartridge The filter cartridge must be replaced as soon as the maximum limiting value set for the ultrapure water is exceeded or when the “Change cartridge” message is shown in the display. Proceed as follows to replace the Filter cartridge: 1. Switch the system off. 2. Shut off the supply of feedwater. 3. Open the dispensing valve until the flow of water stops, then re-close it. 4. Remove the cartridge cover. 5. Disconnect the quick-connects on the feedwater inlet and purified water outlet of the cartridge, then close the inlet and outlet with the stoppers which you have kept for later usage. 6. Draw the used Filter cartridge out from the guide and insert the new Filter cartridge. 7. Remove the stoppers from the new Filter cartridge and store them for later use. 8. Plug the quick-connects correctly onto the new Filter cartridge. 9. Replace the cartridge cover. 10. Open the supply of feedwater. 11. Switch the system on again. 12. Run off and discard at least 5 litres of water. 13. To return the operating time meter to zero, enter the serial number that is given on the cartridge as described in the “Filter cartridge operating hours counter” section. Important: To do this, the system must first be unlocked via the code function, refer here to the "Unlocking the system" section. To air-vent the system, switch it to the „Rinse“ state. 47 Thermo Scientific Barnstead GenPure Ultrapure water system 13.3 Disinfection procedure Disinfection should be regularly carried out, at the latest when the Filter cartridge is replaced. A disinfection cartridge (article no.: 09.2201) is required for disinfection of the system. Use cleaning solutions as follows: MICRO-Chlor Granulate, 1 box, article no. 09.2202 (Europe only) Cleaning Solution, 1 syringe, article no. CMX 25 (US-market only). Please observe the information given in the safety data sheet supplied with Micro-Chlor disinfectant to avoid possible health hazards! Proceed as follows to sanitize your system: 1. Switch the GenPure system off. 2. Shut off the supply of feedwater to the system and open the dispensing valve so that pressure in the system is completely released. 3. Remove the filter cartridge (as under "Changing the filter cartridge" in the Operating Instructions for the system). 4. Unscrew the stopper from the disinfectant cartridge, fill the cartridge with water then empty the contents of a box respectively a syringe of the cleaning solution into the water. Important! For effective disinfection the cartridge must be completely filled with water. 5. Screw the stopper back on the disinfectant cartridge and connect the cartridge in the system (as under "Changing the filter cartridge" in the Operating Instructions for the system). 6. Re-open the feedwater supply. 7. Switch the system on and select the "Disinfection" prompt in the menu. The disinfection programme is finished after approx. 30 minutes. 8. Switch the system off. 9. Shut off the supply of feedwater to the system. 10. Remove the disinfectant cartridge (as under "Changing the filter cartridge" in the Operating Instructions for the system). 11. Connect the new filter cartridge in the system (as under "Changing the filter cartridge" in the Operating Instructions for the system). Before dispensing water from the system, let water run out for approx. 15 minutes. The system is then ready for use. 48 Thermo Scientific Barnstead GenPure Ultrapure water system 49 Thermo Scientific Barnstead GenPure Ultrapure water system 14. Waste disposal When the packaging is no longer needed it can be disposed of as household waste. Systems are in conformity with EEC Guideline 2002/95/EC The system is not to be thrown away as household waste but must be properly disposed of. It can be returned to the manufacturer for safe disposal according to EEC Guideline 2002/96/EC. We therefore request our customers in Germany and other member States in the European Economic Area to contact our local service centre or our headquarters: Thermo Electron LED GmbH Stockland 3 D-56412 Niederelbert, Germany WEEE-Reg.-no.: DE 12471402 In countries outside of the European Economic Area, please contact your local authorities or waste disposal company. 50 Thermo Scientific Barnstead GenPure Ultrapure water system 15. Trouble shouting Fault Cause Remedy System does not start - No power - Connect to power supply No water can be dispensed - Feedwater tap is closed - Feedwater and rinse water connections are the wrong way round - The feedwater pressure is < 0.1 bar - Open the feedwater tap Resistance < 18.2 MΩxcm - System has a UF-module (higher conductivity can occur) - Ion exchange capacity is exhausted - Re-connect them properly - Increase feedwater pressure - Replace the Filter cartridge Control no longer reacts - Incorrect usage - Unplug the line plug for 5 seconds Water leaks out - Hose connections not - Check connections and make watertight them leaktight - Feedwater pressure > 6 bar - Install a downstream pressure reducer Ultrapure water flow rate too low - UF-Module is clogged - Too low a pre-pressure - Internal pressure too low - Replace the UF-module - Increase the pre-pressure - Re-adjust the pressure reducer Wrong time or date - Time difference - Time change - Reset the clock and the date Wrong language - wrong language setting - Correct the language setting Fault message: "Limit value feed“ - Feedwater has too high a conductivity - Limiting value set too low - Check the preatreatment system - Check the limiting value setting and correct it 51 Thermo Scientific Barnstead GenPure Ultrapure water system Fault message: „Limit val. Pure w." - Filter cartridge is exhausted - Limiting value set too low - Replace it with a new one (Art. No.: 09.2005) - Check the limiting value and re-adjust it - The system has a UFmodule (higher conductivity can occur) Fault message: "UV duration" - The maximum operating hours of the UV-lamp have been exceeded - Replace the UV-lamp with a new one (Art. No. 09.2002) and re-set the operating hours counter to zero Fault message: "UV-Intensity" - Intensity to the UV-lamp is no longer sufficient - UV-Sensor is dirtied - Limiting value set too low - Replace the UV-lamp and measure maximum value - Clean the UV-sensor - Check and readjust the limiting value setting Fault message: "Max.temp." - Reduce the temperature by - The temperature in the dispensing water system is too high - Pump interval time too long - Reduce pump interval time - Check and readjust the - Limiting value set too low limiting value setting - Feedwater temperature too - Reduce the feedwater temperature high Fault message: "Meas cell LF1" - Replace the measuring cell - A break in the measuring cell cable - Replace the system control - System control defect - Ultrapure water conductivity - see "Resistance <18.2 MΩxcm" outside the measurement range Fault message: "Meas. cell LF2" - A break in the measuring cell cable - System control defect - Feedwater conductivity outside the measurement range - Replace the measuring cell - A break in the measuring cell cable - System control defect - Replace the measuring cell Fault message: "Meas. cell LF3" 52 - Replace the system control - see Feedwater limiting value - Replace the system control Thermo Scientific Barnstead GenPure Ultrapure water system Fault message: "Temp. meas. cell." Fault message: „change cartridge" - A break in the measuring cell cable - System control defect - Replace the measuring cell - Replace the system control - Operating hours of the filter - Replace it with a new one (Art. No.: 09.2005) cartridge has expired 53 Thermo Scientific Barnstead GenPure Ultrapure water system 16. Replacement parts and consumables 8 11 3 14 1 13 4 12 10 2 6 9 15 7 5 No. Designation 1 2 3 4 5 6 7 8 9 10 11 12 Pressure boosting pump Ultrafiltration module (optional) Filter cartridge Replacement UV-lamp Rinsing solenoid valve Pressure reducer Feedwater conductivity measuring cell Ultrapure water conductivity measuring cell TOC conductivity measuring cell (optional) Check valve 1 bar Microprocessor system control Sterile filter capsule, 0.2 m, for dispensed water 13 UV-Intensity sensor (optional) 14 Dispensing valve 15 Fuse holder for glas tube fuse 5 x 20mm Glas tube fuse 5 x 20mm, 3,15 A, slow fuse Tabletop power pack, 24V DC (not shown) * Wearing part Article- No. 19.0050* 50133980 09.2005 09.2002 50131190* 50133985 16.0126 50133992 50133992 15.0019 50131348 09.1003 16.0222 50133988 50133979 50131758 50134196 We ask for your understanding that we must declare the guarantee given for this system to be invalidated should replacement parts, accessories or consumables from other manufacturers be used, as we have no influence on their quality or appropriateness. 54 Thermo Scientific Barnstead GenPure Ultrapure water system 17. Accessories Designation Disinfection cartridge Disinfection agent, MICRO-Chlor (pack of 12 cans, Europe only) Cleaning Solution, 1 syringe (US-market only) Volume control for water dispensing Printer Qualification Manual IQ, OQ Article- No. 09.2201 09.2202 CMX25 09.2210 09.2207 IOQDOCE50133917 The address to contact when your system requires service: Overview of Thermo Scientific International Sales Organization Postal address USA: Thermo Scientific 275 Aiken Road Asheville, NC 28804 USA Enquiries from USA/Canada Sales: +1 866 984 3766 Service: +1 800 438 4851 Enquiries from Latin America Sales: +1 866 984 3766 Service: +1 866 984 3766 Enquiries from Asia China Sales: +86 10 8419 3588 Service: Toll free 8008105118 Support Mobile 4006505118 or +86 10 8419 3588 India Sales: Service: +91 22 6716 2200 Toll free 1 800 22 8374 or +91 22 6716 2200 Japan Sales: Service: +81 45 453 9220 +81 45 453 9224 Enquiries from the Rest of Asia/Australia/New Zealand Sales: +852 2885 4613 Service: +65 6872 9720 Enquiries from Countries not listed / Rest of EMEA Sales: +49 6184 90 6940 or +33 2 2803 2000 Service: +49 6184 90 6940 Enquiries from Europe Austria Sales: +43 1 801 40 0 Service: +43 1 801 40 0 55 Thermo Scientific Barnstead GenPure Ultrapure water system Belgium Sales: Service: +32 53 73 4241 +32 53 73 4241 Finland/Nordic/Baltic countries Sales: +358 9 329 100 Service: +358 9 329 100 France Sales: Service: +33 2 2803 2180 +33 825 800 119 Germany: Postal Address Germany: Thermo Electron LED GmbH Robert-Bosch-Straße 1 D - 63505 Langenselbold Phone Sales: E-Mail: Toll free 0800 1 536 376 or +49 6184 90 6940 Toll free 0800 1 112110 or +49 6184 90 6940 [email protected] Italy Sales: Service: +39 02 95059 341 +39 02 95059 250 Service: Netherlands Sales: +31 76 579 5555 Service: +31 76 579 5639 Russa/CIS Sales: Service: +7 812 703 4215 +7 812 703 4215 Spain/Portugal Sales: +34 93 223 0918 Service: +34 93 223 0918 Switzerland Sales: Service: +41 44 454 1212 +41 44 454 1212 UK/Ireland Service: Sales: +44 870 609 9203 +44 870 609 9203 56 Thermo Scientific Barnstead GenPure Ultrapure water system 18. Terminal assignment 57 Thermo Scientific Barnstead GenPure Ultrapure water system 58 Thermo Scientific Barnstead GenPure Ultrapure water system 19. Maintenance record (Please carefully keep this record, as complete and correct entries are a requirement for the validity of the guarantee) Customer address: Location: Type of system: Serial number: Year made: Date Last change of Filter cartridge Feedwater resistance Ultrapure water resistance [MΩxcm] [MΩxcm] Last cleaning / disinfection Ultrapure water flow rate [L/h] Last change Remarks of pretreatment Tempe rature [°C] TOC-value UVIntensity [ppb] [%] UV-Lamp operating hours [h] Signature Any false entry is a falsification of documents. The following points are to be observed to ensure maintenance of the quality of the system:  1x/ Weekly – record measured values For the optimal ultrapure water to be produced, the feedwater pre-treatment must be checked and subject to maintenance at regular intervals. 59 Thermo Scientific Barnstead GenPure Ultrapure water system Contact Information Thermo Scientific North America: USA/Canada +1 866 984 3766 (866-9-THERMO) Europe: Austria +43 1 801 40 0, Belgium +32 53 73 42 41, France +33 2 2803 2180, Germany national toll free 08001-536 376, Germany international +49 6184 90 6940, Italy +39 02 95059 448, Netherlands +31 76 579 55 55, Nordic/Baltic/CIS countries +358 9 329 10200, Russia +7 812 703 42 15, Spain/Portugal +34 93 223 09 18, Switzerland +41 44 454 12 12, UK/Ireland +44 870 609 9203 Asia: Australia +61 39757 4300, China +86 21 6865 4588 or +86 10 8419 3588, India toll free 1800 22 8374, India +91 22 6716 2200, Japan +81 45 453 9220, New Zealand +64 9 980 6700, Other Asian countries +852 2885 4613 Countries not listed: +49 6184 90 6940 © 2011 Thermo Fisher Scientific Inc. All rights reserved. All trademarks are the property of Thermo Fisher Scientific Inc. and its subsidiaries. Specifications, terms and pricing are subject to change. Not all products are available in all countries. Please consult your local sales representative for details. 60