Transcript
Rotavapor ® R-210 / R-215 Technical data sheet The evaporation of solvents is a routine process widely performed in the laboratory. It is therefore important that the instruments optimally support the user’s working methods and match to the conditions and needs of the laboratory.
Scope of delivery All models are delivered ready to use and are complete of: Components
System with glass
System w/o glass
Rotavapor® (according to order code)
1
1
Heating bath
1
(1)
Condenser (according to order code)
1
-
Vapor duct (with Combi-Clip)
1
-
Vacuum seal (WD26)
1
-
Evaporating flask (1 liter)
1
-
Receiving flask (1 liter)
1
-
Flyer "List of solvents"
1
1
Flask holder
1
1
Vapor temperature sensor
(1)*
-
Stage probe
( 1 ) **
-
* Only delivered if R-215 system is ordered with glass assembly V, S, E or BY ** Only delivered if system is ordered with Vacuum Controller V-855 and glass assemly V or S
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Order code Choose the configuration according to your needs: Systems with glass
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Rotavapor R-210 / R-215 0 R-210 without display 1 R-215 with display for rotation speed and vapor temperature 2 R-210 without heating bath *** 3 R-215 without heating bath ***
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Voltage options 1 220 - 240 V *** 2 100 - 120 V Joint options for evaporating flask 1 SJ 29/32 2 SJ 24/40 3 SJ 29/42
Vacuum controller 0 Without controller 1 Vacuum Controller V-850 2 Vacuum Controller V-855 Valve unit 0 Without valve unit 1 Woulff bottle for vacuum controller (needed for stand-alone system with V-700) 2 Valve unit for vacuum controller (not necessary in stand-alone system with V-700)
Glass assembly options A Glass assembly A V Glass assembly V */** C Glass assembly C S Glass assembly S */** E Glass assembly E * R Glass assembly CR Y Glass assembly BY P+G 0 Without coating 1 With safety coating
* Vapor temperature measurement possible ** Auto-distillation possible *** The Rotavapor without the heating bath supports the whole voltage range of 100 - 240 V. Therefore when ordering a system without heating bath the voltage option 100 - 120 V needs to be chosen
Systems without glass
2
3
0
2
0
N
0
0
0
R-210 with bath, w/o glass, 100 - 120 V
2
3
0
1
0
N
0
0
0
R-210 with bath, w/o glass, 220 - 240 V
2
3
2
0
0
N
0
0
0
R-210 w/o bath, w/o glass, 100 - 240 V
2
3
1
2
0
N
0
0
0
R-215 with bath, w/o glass, 100 - 120 V
2
3
1
1
0
N
0
0
0
R-215 with bath, w/o glass, 220 - 240 V
2
3
3
0
0
N
0
0
0
R-215 w/o bath, w/o glass, 100 - 240 V
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Order code for Rotavapor systems with vacuum pump, vacuum controller and optional recirculating chiller.
2
3
1 Rotavapor R-210 / R-215 0 R-210 without display 1 R-215 with display for rotation speed and vapor temperature Voltage options 1 220 - 240 V 2 100 - 120 V
Vacuum controller 1 Vacuum Controller V-850 2 Vacuum Controller V-855 (for automatic distillation) Vacuum pump options 1 Vacuum Pump V-700 (1.8 m3/h, <10 mbar) 2 Vacuum Pump V-700 with secondary condenser 4 Vacuum Pump V-710 (3.1 m3/h, 2 mbar) 5 Vacuum Pump V-710 with secondary condenser
Joint options for evaporating flask 1 SJ 29/32 2 SJ 24/40 Glass assembly options A Glass assembly A V Glass assembly V */** C Glass assembly C S Glass assembly S */** P+G 0 Without coating 1 With safety coating
Recirculating chiller 0 Without recirculating chiller 1 Recirculating Chiller F-100 (fix 10 °C, 500 W) 2 Recirculating Chiller F-105 (-10 °C to 25 °C, 500 W) 3 Recirculating Chiller F-108 (-10 °C to 25 °C, 800 W) * When ordering with V-855, the stage probe is included ** When ordering with a R-215, the vapor temperature sensor is included
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Description of glass assemblies Abbr.
Type / Application
Cooling surface area
V
Vertical condenser
0.146 m2
For standard applications. The most common condenser and in combination with an R-215 this glass assembly is equipped with a vapor temperature sensor.
C
Dry ice condenser (cold trap)
0.05 m2
For distillation of solvents with low boiling points. No cooling water is necessary.
A
Diagonal condenser
0.146 m2
For standard applications where height is limited.
S
Vertical reflux condenser with shut-off valve
0.146 m2
For distillation under reflux. In combination with an R-215 this glass assembly is equipped with a vapor temperature sensor.
CR
Dry ice reflux condenser with shut-off valve
0.05 m2
For distillation under reflux of solvents with low boiling points. No cooling water is needed.
E
Descending condenser with expansion vessel
0.148 m2
For foaming and bumping products. In combination with an R-215, this glass assembly is equipped with a vapor temperature sensor.
BY
Double jacket vertical reflux condenser with shut-off valve
0.125 m2
For distillation and reflux operation. There is an additional SJ 29/32 joint on top for flexible expansion. In combination with an R-215, this glass assembly is equipped with a vapor temperature sensor.
Dimensions Dimension (WxHxD) Rotavapor R-210 / R-215 with V-condenser
590 x 840 x 420 mm
Rotavapor R-210 / R-215 w/o condenser
550 x 575 x 420 mm
Technical data Rotavapor ® R-210
Rotavapor ® R-215
Weight (depending on glass assembly)
16 - 18 kg
16 - 18 kg
Operating voltage
100 - 240 V
100 - 240 V
Frequency
50/60 Hz
50/60 Hz
Power consumption
60 W
60 W
IP class
21
21
Angle adjustable
0 - 25 °
0 - 25 °
Stroke distance
145 mm
145 mm
Rotation speed
20 - 280 rpm
20 - 280 rpm
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Rotavapor ® R-210
Rotavapor ® R-215
Flask size range *
50 - 4000 mL
50 - 4000 mL
Maximum flask capacity
3 kg
3 kg
Display
None
Rotation speed and vapor temperature
Approval
CE / CSA
CE / CSA
Heating Bath B-491
Heating Bath B-495
Dimension (WxHxD)
285 x 240 x 300 mm
310 x 230 x 320 mm
Weight
4 kg
5 kg
Operating voltage
100 - 120 V or 220 - 240 V
100 - 120 V or 220 - 240 V
Frequency
50/60 Hz
50/60 Hz
Power consumption
1700 W
1700 W
Heating power
1300 W
1300 W
IP class
21
21
Controlled temperature range
20 - 180 °C (water and oil)
20 - 95 °C
Digital display
Set and actual temperature
Set and actual temperature
Kettle connector between bath base and heating bath
Yes
Yes
Infrared communication
Yes
Yes
Heating bath temperature lock
Yes
Yes
Temperature deviation
± 2 °C
± 3 °C
Max. flask size
4000 mL
5000 mL
Approval
CE / CSA
CE / CSA
* using Heating Bath B-491
Complementary products See respective product brochures, and technical data sheets for more information. Chiller F-100
Chiller F-105
Chiller F-108
Pump V-700
Pump V-710
Controller V-850
Controller V-855
R-210 / R-215
autonomous
manually controlled
manually controlled
autonomous
autonomous
for pump/ chiller only
for pump/ chiller only
R-210 / R-215 with V-850 / V-855
autonomous
controlled
controlled
controlled
controlled
-
-
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Exemplary solution The following items are listed based on two solutions, shown in the “Laboratory Evaporation Solutions“-brochure. Solution “Rotavapor ® Semi-Automated”
Order number
Rotavapor® R-210, V-condenser, SJ 29/32, P+G safety coating (220 - 240 V), Vacuum Controller V-850, Vacuum Pump V-700, Recirculating Chiller F-105
23011V11112
Safety shield
048052
Solution “Rotavapor ® Automated”
Order number
Rotavapor® R-215, V-condenser, SJ 29/32, auto-distillation (220 - 240 V), Vacuum Controller V-855, Vacuum Pump V-700, Recirculating Chiller F-105, stage probe (for auto-distillation)
23111V02112
Distillation Record software
051480
Rotavapor accessories Order number Manometer with needle valve
047291
For manual regulation of vacuum when using house vacuum. Includes holder
Stop-position extension
044466
Extension of end-stop rod to stop the automatic lift at a higher level (for large flasks with the B-495)
Flask holder
048618
Keeps the flask stable on the table, made of non-slipping EPDM
Set flask holder, 5 pcs.
11059916
Keeps the flask stable on the table, made of non-slipping EPDM
Vacuum seal WD26
048021
Low abrasion vacuum seal in PTFE composite material
Laboratory grease Glisseal (blue)
048197
Tube 60 g
Water jet pump unit B-764, 24 V
031358
Simple principle of vacuum generation, without cooling water valve, 24 V (1 magnetic valve and a FFKM backstroke valve). Only in combination with Vacuum Controller
Water jet pump unit B-767, 24 V
031357
Simple principle of vacuum generation, with cooling water valve, 24 V (2 magnetic valve and a FFKM backstroke valve). Only in combination with Vacuum Controller
Cooling water valve
031356
Save water as the vacuum controller opens the cooling water feed only during distillation, 24 V
Standard stop-cock, SJ 18.8/38
040627
For aeration
Classic stop-cock, SJ 18.8/38
000637
For aeration, less cross-contamination than standard stop-cock (040627).
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Order number Stop-cock PTFE, SJ 18.8/38
023896
For applications where grease should be avoided. Used instead of standard stop- cock (040627).
Condensor holder complete
048180
Fits glass assemblies V, C, S and CR
Rotavapor heating bath For R-210 / R-215
Order number
Heating Bath B-491, 20 – 180 °C, max. flask size 4000 mL Complete, including base with power supply
220 – 240 V
048200
100 – 120 V
048201
220 – 240 V (gold-coated) *
048277
Heating Bath B-495, 20 – 95 °C, max. flask size 5000 mL Complete, including base with power supply, bath replenishment
220 – 240 V
048240
100 – 120 V
048241
220 – 240 V (gold-coated) *
048246
For R-200 / R-205
Order number
Heating Bath B-491, 20 – 180 °C, max. flask size 4000 mL Complete, including base with power supply
220 – 240 V
048212
100 – 120 V
048213
220 – 240 V (gold-coated) *
046585
Base plate for R-200 / R-205 Special platform adapter for Heating Bath B-491 and B-495
220 – 240 V
048358
100 – 120 V
048359
For R-114
Order number
Heating Bath B-491, 20 – 180 °C, max. flask size 4000 mL Complete, including base with power supply
220 – 240 V
047374
100 – 120 V
047375
* The contacts on both sides of the kettle connector are gold coated which are especially resistant against corrosion found in very harsh environments
Heating bath accessories
Order number
Protective shield for B-491
048052
Effective user protection against splashing and implosions
Protective shield for B-495
048245
Effective user protection against splashing and implosions
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Heating bath accessories
Order number
Top cover for heating bath B-491
048230
To cover bath with a lid when not in use to safe energy and less evaporation of heating medium
Floating balls, 450 pcs.
036405
To reduce energy consumption of the heating bath (up to 100 °C, PP) and less evaporation of heating medium
Rotavapor glass assemblies The following items only have to be ordered when system without glass is ordered. Order number Glass assembly V complete
040600
Includes receiving flask (1 liter), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly V complete P+G safety coating
040602
Includes receiving flask (1 liter, P+G safety coating), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly C complete
040640
Includes receiving flask (1 liter), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly C complete P+G safety coating
040642
Includes receiving flask (1 liter, P+G safety coating), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Cooling coil insert, replaces cold finger
027488
Includes the insert and the cold trap seal (PTFE-ring with 2 O-rings) and is used like a normal liquid-cooled condenser.
Glass assembly A complete
048168
Includes receiving flask (1 liter), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly A complete P+G safety coating
048169
Includes receiving flask (1 liter, P+G safety coating), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly S complete
040650
Includes receiving flask (1 liter), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly S complete P+G safety coating
040652
Includes receiving flask (1 liter, P+G safety coating), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Soxhlet extraction unit, 200 mL
011744
For extractions in combination with glass assembly S
Soxhlet extraction unit, 500 mL
011745
For extractions in combination with glass assembly S
Extraction cartridges, 1 x 200 mL
008560
Extraction cartridges, 1 x 500 mL
000989
Extraction cartridges, 25 x 200 mL
018106
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Order number Glass assembly CR complete P+G safety coating
040672
Includes receiving flask (1 liter, P+G safety coating), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly E complete
040660
Includes receiving flask (1 liter), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly E complete P+G safety coating
040662
Includes receiving flask (1 liter, P+G safety coating), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Glass assembly BY complete
048176
Includes receiving flask (1 liter), required hoses and ball joint clamp, does not include evaporating flask and vapor duct.
Rotavapor glass accessories All vapor ducts include Combi-Clip Vapor duct compatible with WD26
SJ 29/32
SJ 24/40
SJ 29/42
SJ 34/35
Vapor duct for glass assembly A (285 mm)
048164
048165
048166
048167
Vapor duct for glass assembly C and V
048160
048161
048162
048163
050560
050561
050562
050563
SJ 24/29
044444
(177 - 190 mm) Analytic* Vapor duct for glass assembly C and V (200 - 210 mm)
Vapor duct compatible with KD22
SJ 29/32
Vapor duct for glass assembly C and V (180 mm)
045650
Additional glassware Additional glassware like evaporating flasks, drying flasks, receiving flasks, beaker flasks, Reitmeyer adapters (bump traps) and distillation spiders can be found in the glassware brochure.
www.buchi.com/laboratory-evaporation
Quality in your hands
R-210 R-215 Data Sheet en 1401 D / Technical data are subject to change without notice / Quality Systems ISO 9001 The English version is the original language version and serves as basis for all translations into other languages.
*there is no liquid flowing back into the evaporating flask
